Extraction and Characterization of Silica from Reeds Biomass (Imperata cylindrical) in Various Annealing Temperature

Authors

  • Dyah Ayu Pramoda Wardani Department of Chemistry, Faculty of Mathematics and Natural Science, University of Palangka Raya, Palangka Raya 73111, Central Kalimantan, Indonesia http://orcid.org/0000-0001-9460-4937
  • Neny Kurniawati Department of Physics, Faculty of Mathematics and Natural Science, University of Palangka Raya, Palangka Raya 73111, Central Kalimantan, Indonesia http://orcid.org/0000-0001-8740-0039
  • Budi Hariyanto Department of Physics, Faculty of Mathematics and Natural Science, University of Palangka Raya, Palangka Raya 73111, Central Kalimantan, Indonesia http://orcid.org/0000-0002-6403-0693
  • Nazopatul Patonah Har Department of Physics, Faculty of Mathematics and Natural Science, IPB University, Bogor 16680, West Java, Indonesia
  • Noviyan Darmawan Department of Chemistry, Faculty of Mathematics and Natural Science, IPB University, Bogor 16680, West Java, Indonesia http://orcid.org/0000-0002-0197-6094
  • Rofiqul Umam School of Science and Technology, Kwansei Gakuin University, Japan http://orcid.org/0000-0002-7095-5967
  • Irzaman Irzaman Department of Physics, Faculty of Mathematics and Natural Science, IPB University, Bogor 16680, West Java, Indonesia http://orcid.org/0000-0002-6447-3726

DOI:

https://doi.org/10.4302/plp.v15i1.1186

Keywords:

Reeds biomass, annealing temperature, cristoballite, band gap energy, optical properties, dielectric function

Abstract

Reeds biomass has been successfully extracted. It calcinated with annealing temperatures at 800 °C (A800), 850 °C (A850), and 900 °C (A900). The x-ray pattern showed that it has a cristoballite (SiO2) crystal structure. The band gap energy values are 3.8 eV, 3.7 eV and 4.7 eV, respectively. FTIR spectra show the groups are silanol, siloxane, and monohydride. Quantitatively, it provide results to determine the optical properties and dielectric functions which indicate shift to longer wavelengths with an increase in annealing temperature. The morphology gives different image where the particles are formed flakes (A800), aggregates (A850) and porous aggregates (A900).

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References

  1. A. F. Ramdja, R. A. Silalahi, N. Sihombing, "Pengaruh waktu, temperatur dan dosis H2SO4 pada hidrolisa asam terhadap kadar etanol berbahan baku alang-alang," J. Tek. Kim., 17, (2010). CrossRef
  2. Z. S. Osvaldo, P. Putra, M. Faizal, "Pengaruh konsentrasi asam dan waktu pada proses hidrolisis dan fermentasi pembuatan bioetanol dari alang-alang," J. Tek. Kim., 18, (2012). CrossRef
  3. I. S. Naji, N. A. Khalifa, and H. M. Khalaf, "Influence of annealing temperature on the physical properties of thin Cu2SiO4 films prepared by pulsed laser deposition," Dig. J. Nanomater. Biostructures, 12, 899 (2017). DirectLink
  4. M. Sahri, A. R. Tualeka, N. Widajati, "Quantitative risk assesment of crystalline silica exposure in ceramics industry," Indian J. Public Heal. Res. & Dev., 10, 601 (2019). CrossRef
  5. A. Berendjchi, R. Khajavi, M. E. Yazdanshenas, "Application of nanosols in textile industry," Int. J. Green Nanotechnol., 1, 1943089213506814 (2013). CrossRef
  6. P. Y. Steinberg, "Structural and mechanical properties of silica mesoporous films synthesized using deep X-rays: implications in the construction of devices," Front. Mater., 8, 27 (2021). CrossRef
  7. A. F. Lourenço, J. A. F. Gamelas, J. Sequeira, P. J. Ferreira, J. L. Velho, "Improving paper mechanical properties using silica-modified ground calcium carbonate as filler," BioResources, 10, 8312 (2015). CrossRef
  8. S. Begum, M. Allaudin, M. A. Qaiser, and F. KHAN, "Beneficiation of silica sand for the manufacturing of optical glass". J.Chem. Soc. Pakistan, 21, 83 (1999). DirectLink
  9. N. H. N. A. Hadi, A. Anuar, R. K. Shuib, "Effect of Different Salinization Methods of Silica Filler on Rubber Reinforcement," J. Eng., 15, 71 (2019). CrossRef
  10. K. Kayed and D. B. Kurd, "The effect of annealing temperature on the structural and optical properties of Si/SiO2 composites synthesized by thermal oxidation of silicon wafers," Silicon, 14, 5157 (2021). CrossRef
  11. F. Ravaux, N. S. Rajput, J. Abed, L. George, M. Tiner, M. Jouiad, "Effect of rapid thermal annealing on crystallization and stress relaxation of SiGe nanoparticles deposited by ICP PECVD," RSC Adv.,7, 32087 (2017). CrossRef
  12. H. Liu et al., "Design and synthesis of carbon-coated α-Fe2O3-Fe3O4 heterostructured as anode materials for lithium ion batteries," Appl. Surf. Sci., 495, 143590 (2019). CrossRef
  13. M. Ghasemifard, E. Fathi, M. Ghamari, "The effect of Fe3+-doped on structure and optical properties of mesoporous Al2O3/SiO2 composite," Mater. Sci. Semicond. Process., 42, 349 (2016). CrossRef
  14. X. Lu et al., "Effect of high-intensity ultrasound irradiation on the stability and structural features of coconut-grain milk composite systems utilizing maize kernels and starch with different amylose contents," Ultrason. Sonochem., 55, 135 (2019). CrossRef
  15. E. W. Juni, A. Arnelli, S. Sriatun, "Pemanfaatan Surfaktan Kationik Hasil Sublasi sebagai Molekul Pengarah pada Pembuatan Material Berpori dari Sekam Padi," J. Kim. Sains dan Apl., 15, 24 (2012). CrossRef
  16. F. Adam, K. Kandasamy, S. Balakrishnan, "Iron incorporated heterogeneous catalyst from rice husk ash," J. Colloid Interface Sci., 304, 137 (2006). CrossRef
  17. K. C. Wong, "Review of spectrometric identification of organic compounds." J. Chem. Educ., 92, 1602 (2015). CrossRef
  18. L. H. Abuhassan, "Enhancement of the production yield of fluorescent silicon nanostructures using silicon-based salts," Sains Malaysiana, 39, 837 (2010). DirectLink
  19. U. Kalapathy, A. Proctor, J. Shultz, "Silica xerogels from rice hull ash: structure, density and mechanical strength as affected by gelation pH and silica concentration", J. Chem. Technol. & Biotechnol., 75, 464 (2000) CrossRef

Author Biography

Dyah Ayu Pramoda Wardani, Department of Chemistry, Faculty of Mathematics and Natural Science, University of Palangka Raya, Palangka Raya 73111, Central Kalimantan, Indonesia

Department of Chemistry

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Published

2023-04-02

How to Cite

[1]
D. A. P. Wardani, “Extraction and Characterization of Silica from Reeds Biomass (Imperata cylindrical) in Various Annealing Temperature”, Photonics Lett. Pol., vol. 15, no. 1, pp. 4–6, Apr. 2023.

Issue

Vol. 15 No. 1 (2023)

Section

Articles

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